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高速机械粉磨对油基钻屑灰渣活性的影响
Effect of high-speed mechanical grinding on activity of oil-based drilling cuttings ash
2024年第2期
高速机械粉磨;油基钻屑灰渣;活性激发;胶砂;性能
High-speed mechanical grinding; Oil-based drilling cuttings ash; Active excitation; Mortar; Performance
2024年第2期
10.19761/j.1000-4637.2024.02.088.05
国家科技重大专项课题项目(2016ZX05040006-001-011);国家自然科学基金项目(51108393)。
张显河1,文 华1,*,郑 召1,包志涛1,余伟豪2,雷 旭1,范 伟1
1.西南科技大学 土木工程与建筑学院,四川 绵阳621010;2.沈阳建筑大学 土木工程学院, 辽宁 沈阳110168

张显河1,文 华1,*,郑 召1,包志涛1,余伟豪2,雷 旭1,范 伟1

张显河,文华,郑召,等.高速机械粉磨对油基钻屑灰渣活性的影响[J].混凝土与水泥制品,2024(2):88-92.

ZHANG X H,WEN H,ZHENG Z,et al.Effect of high-speed mechanical grinding on activity of oil-based drilling cuttings ash[J].China Concrete and Cement Products,2024(2):88-92.

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摘   要:对油基钻屑灰渣进行了高速机械粉磨处理,研究了粉磨时间(0~7 min)对灰渣粒径分布和比表面积的影响,分析了掺灰渣胶砂试件的力学性能,并进行了XRD、SEM、FTIR微观分析。结果表明:与未粉磨处理的灰渣相比,粉磨3 min灰渣的粒径分布范围缩小至1.220~40.100 μm,D50降低了60.9%,比表面积增大了27.6%;与其他粉磨时间的灰渣相比,用粉磨3 min的灰渣等质量取代30%水泥所制备的胶砂试件的28 d抗压强度最高,28 d抗折强度也较高;适宜的粉磨时间能够促进灰渣中的活性SiO2、Al2O3等与水泥水化产物Ca(OH)2发生二次水化反应,生成C-S-H凝胶和AFt,提高胶砂结构的密实度。 Abstract: High-speed mechanical grinding treatment was carried out on oil-based drilling cuttings ash, and the effect of grinding time(0~7 min) on the particle size distribution and specific surface area of the oil-based drilling cuttings ash was studied. The mechanical properties of the mortar specimens mixed with oil-based drilling cuttings ash were analyzed, and XRD, SEM and FTIR microscopic analysis were conducted. The results show that compared with the oil-based drilling cuttings ash without grinding treatment, the particle size distribution range of the oil-based drilling cuttings ash after grinding for 3 min is reduced to 1.220~40.100 μm, the D50 is decreased by 60.9%, and the specific surface area is increased by 27.6%. Compared with the oil-based drilling cuttings ash from other grinding times, the 28 d compressive strength of the mortar specimens prepared by replacing 30% cement with oil-based drilling cuttings ash from grinding for 3 min is the highest, and the 28 d flexural strength is high. The appropriate grinding time can promote the secondary hydration reaction between the active SiO2, Al2O3, etc. in the oil-based drilling cuttings ash and the cement hydration product Ca(OH)2 to generate C-S-H gel and AFt, thus improving the structural compactness of the mortar.
英文名 : Effect of high-speed mechanical grinding on activity of oil-based drilling cuttings ash
刊期 : 2024年第2期
关键词 : 高速机械粉磨;油基钻屑灰渣;活性激发;胶砂;性能
Key words : High-speed mechanical grinding; Oil-based drilling cuttings ash; Active excitation; Mortar; Performance
刊期 : 2024年第2期
DOI : 10.19761/j.1000-4637.2024.02.088.05
文章编号 :
基金项目 : 国家科技重大专项课题项目(2016ZX05040006-001-011);国家自然科学基金项目(51108393)。
作者 : 张显河1,文 华1,*,郑 召1,包志涛1,余伟豪2,雷 旭1,范 伟1
单位 : 1.西南科技大学 土木工程与建筑学院,四川 绵阳621010;2.沈阳建筑大学 土木工程学院, 辽宁 沈阳110168

张显河1,文 华1,*,郑 召1,包志涛1,余伟豪2,雷 旭1,范 伟1

张显河,文华,郑召,等.高速机械粉磨对油基钻屑灰渣活性的影响[J].混凝土与水泥制品,2024(2):88-92.

ZHANG X H,WEN H,ZHENG Z,et al.Effect of high-speed mechanical grinding on activity of oil-based drilling cuttings ash[J].China Concrete and Cement Products,2024(2):88-92.

摘要
参数
结论
参考文献
引用本文

摘   要:对油基钻屑灰渣进行了高速机械粉磨处理,研究了粉磨时间(0~7 min)对灰渣粒径分布和比表面积的影响,分析了掺灰渣胶砂试件的力学性能,并进行了XRD、SEM、FTIR微观分析。结果表明:与未粉磨处理的灰渣相比,粉磨3 min灰渣的粒径分布范围缩小至1.220~40.100 μm,D50降低了60.9%,比表面积增大了27.6%;与其他粉磨时间的灰渣相比,用粉磨3 min的灰渣等质量取代30%水泥所制备的胶砂试件的28 d抗压强度最高,28 d抗折强度也较高;适宜的粉磨时间能够促进灰渣中的活性SiO2、Al2O3等与水泥水化产物Ca(OH)2发生二次水化反应,生成C-S-H凝胶和AFt,提高胶砂结构的密实度。

Abstract: High-speed mechanical grinding treatment was carried out on oil-based drilling cuttings ash, and the effect of grinding time(0~7 min) on the particle size distribution and specific surface area of the oil-based drilling cuttings ash was studied. The mechanical properties of the mortar specimens mixed with oil-based drilling cuttings ash were analyzed, and XRD, SEM and FTIR microscopic analysis were conducted. The results show that compared with the oil-based drilling cuttings ash without grinding treatment, the particle size distribution range of the oil-based drilling cuttings ash after grinding for 3 min is reduced to 1.220~40.100 μm, the D50 is decreased by 60.9%, and the specific surface area is increased by 27.6%. Compared with the oil-based drilling cuttings ash from other grinding times, the 28 d compressive strength of the mortar specimens prepared by replacing 30% cement with oil-based drilling cuttings ash from grinding for 3 min is the highest, and the 28 d flexural strength is high. The appropriate grinding time can promote the secondary hydration reaction between the active SiO2, Al2O3, etc. in the oil-based drilling cuttings ash and the cement hydration product Ca(OH)2 to generate C-S-H gel and AFt, thus improving the structural compactness of the mortar.

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(1)随着粉磨时间的增加,灰渣的粒径分布范围基本呈先减小后增大趋势,比表面积基本呈先快速增大后缓慢增大趋势,推荐粉磨时间为3 min。
(2)与掺未粉磨灰渣的试件相比,掺粉磨灰渣试件的28 d抗压、抗折强度均较高,其中,掺粉磨3 min灰渣试件的28 d抗压强度最高,28 d抗折强度也较高。
 (3)高速机械粉磨有效提高了灰渣的活性,促进了灰渣中的SiO2、Al2O3玻璃体网络结构解聚,并与水泥水化产物Ca(OH)2发生二次水化反应,生成C-S-H凝胶和AFt晶体,从而使胶砂结构更加密实。但过长的粉磨时间会导致灰渣颗粒因过细而发生团聚,从而影响其二次水化反应。

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张显河,文华,郑召,.高速机械粉磨对油基钻屑灰渣活性的影响[J].混凝土与水泥制品,2024(2):88-92.

ZHANG X H,WEN H,ZHENG Z,et al.Effect of high-speed mechanical grinding on activity of oil-based drilling cuttings ash[J].China Concrete and Cement Products,2024(2):88-92.

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